Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P–E···Te(II,IV) Bonding Situations (E = O, S, Se)
Authors of publication
Hupf, Emanuel; Do, Truong Giang; Nordheider, Andreas; Wehrhahn, Maren; Sanz Camacho, Paula; Ashbrook, Sharon E.; Lork, Enno; Slawin, Alexandra M. Z.; Mebs, Stefan; Woollins, J. Derek; Beckmann, Jens
Journal of publication
Organometallics
Year of publication
2017
a
10.9986 ± 0.0002 Å
b
18.2471 ± 0.0004 Å
c
18.4685 ± 0.0004 Å
α
90°
β
104.559 ± 0.001°
γ
90°
Cell volume
3587.47 ± 0.13 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
6
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0257
Residual factor for significantly intense reflections
0.018
Weighted residual factors for significantly intense reflections
0.0325
Weighted residual factors for all reflections included in the refinement
0.034
Goodness-of-fit parameter for all reflections included in the refinement
