Pyramidanes: The Covalent Form of the Ionic Compounds
Authors of publication
Lee, Vladimir Ya.; Gapurenko, Olga A.; Ito, Yuki; Meguro, Takahiko; Sugasawa, Haruka; Sekiguchi, Akira; Minyaev, Ruslan M.; Minkin, Vladimir I.; Herber, Rolfe H.; Gornitzka, Heinz
Journal of publication
Organometallics
Year of publication
2016
Journal volume
35
Journal issue
3
Pages of publication
346
a
12.7913 ± 0.0008 Å
b
12.8192 ± 0.0008 Å
c
16.8594 ± 0.0011 Å
α
68.348 ± 0.001°
β
87.935 ± 0.001°
γ
76.584 ± 0.001°
Cell volume
2495.6 ± 0.3 Å3
Cell temperature
150 ± 2 K
Ambient diffraction temperature
150 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0341
Residual factor for significantly intense reflections
0.0332
Weighted residual factors for significantly intense reflections
0.0867
Weighted residual factors for all reflections included in the refinement
0.0874
Goodness-of-fit parameter for all reflections included in the refinement
