Information card for entry 4088520

Structure parameters

• Common name: hannr02
• Formula: C27 H63 Sb Si6
• Calculated formula: C27 H63 Sb Si6
• Title of publication: Mechanochemical Influence on the Stereoselectivity of Halide Metathesis: Synthesis of Group 15 Tris(allyl) Complexes
• Authors of publication: Rightmire, Nicholas R.; Bruns, David L.; Hanusa, Timothy P.; Brennessel, William W.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 1698
• a: 10.643 ± 0.004 Å
• b: 10.792 ± 0.004 Å
• c: 20.226 ± 0.007 Å
• α: 81.289 ± 0.007°
• β: 89.569 ± 0.007°
• γ: 61.724 ± 0.006°
• Cell volume: 2016.8 ± 1.3 ų
• Cell temperature: 100 ± 0.5 K
• Ambient diffraction temperature: 100 ± 0.5 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0864
• Residual factor for significantly intense reflections: 0.0675
• Weighted residual factors for significantly intense reflections: 0.1557
• Weighted residual factors for all reflections included in the refinement: 0.1657
• Goodness-of-fit parameter for all reflections included in the refinement: 1.123
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No