Information card for entry 4088528

Structure parameters

• Formula: C29 H46 Cl P2 Rh
• Calculated formula: C29 H46 Cl P2 Rh
• SMILES: C12c3c(cccc3)[P](C(C)(C)C)(C(C)(C)C)[RhH]2(Cl)[P](c2c1cccc2)(C(C)(C)C)C(C)(C)C
• Title of publication: Ligand Attachment Chemistry in the Preparation of PCsp3P and PCsp2P Complexes of Rhodium
• Authors of publication: Logan, Jessamyn R.; Piers, Warren E.; Borau-Garcia, Javier; Spasyuk, Denis M.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 9
• Pages of publication: 1279
• a: 17.469 Å
• b: 12.732 Å
• c: 15.832 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3521.28 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0247
• Residual factor for significantly intense reflections: 0.0241
• Weighted residual factors for significantly intense reflections: 0.0611
• Weighted residual factors for all reflections included in the refinement: 0.0614
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No