Information card for entry 4088543

Structure parameters

• Formula: C18.5 H28 Br0.5 Ge Mn0.5 N2 O1.5
• Calculated formula: C18.5 H28 Br0.5 Ge Mn0.5 N2 O1.5
• Title of publication: [MnBrL(CO)4] (L = Amidinatogermylene): Reductive Dimerization, Carbonyl Substitution, and Hydrolysis Reactions
• Authors of publication: Cabeza, Javier A.; García-Álvarez, Pablo; Gobetto, Roberto; González-Álvarez, Laura; Nervi, Carlo; Pérez-Carreño, Enrique; Polo, Diego
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 11
• Pages of publication: 1761
• a: 10.4964 ± 0.0002 Å
• b: 17.1705 ± 0.0003 Å
• c: 12.3471 ± 0.0002 Å
• α: 90°
• β: 111.44 ± 0.002°
• γ: 90°
• Cell volume: 2071.31 ± 0.07 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0288
• Residual factor for significantly intense reflections: 0.0241
• Weighted residual factors for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.0565
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No