Information card for entry 4088726

Structure parameters

• Formula: C66 H84 Cl3 Ge3 N6
• Calculated formula: C66 H84 Cl3 Ge3 N6
• Title of publication: Synthesis of Trinuclear Tin(II), Germanium(II), and Aluminum(III) Cyclophane Complexes
• Authors of publication: Ermert, David M.; Gordon, Jesse B.; Abboud, Khalil A.; Murray, Leslie J.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 21
• Pages of publication: 3651
• a: 44.808 ± 0.003 Å
• b: 18.1308 ± 0.0013 Å
• c: 15.9563 ± 0.0011 Å
• α: 90°
• β: 100.879 ± 0.0012°
• γ: 90°
• Cell volume: 12730 ± 1.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0395
• Residual factor for significantly intense reflections: 0.0304
• Weighted residual factors for significantly intense reflections: 0.0815
• Weighted residual factors for all reflections included in the refinement: 0.0853
• Goodness-of-fit parameter for all reflections included in the refinement: 1.042
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No