Information card for entry 4088763

Structure parameters

• Common name: DippBF3
• Formula: C34.5 H42 B Cl F4 N3 O3 Re
• Calculated formula: C34.5 H42 B Cl F4 N3 O3 Re
• Title of publication: Reductive Carbonylation of Oxorhenium Hydrides Induced by Lewis Acids
• Authors of publication: Lambic, Nikola S.; Lilly, Cassandra P.; Robbins, Leanna K.; Sommer, Roger D.; Ison, Elon A.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 17
• Pages of publication: 2822
• a: 9.1424 ± 0.0003 Å
• b: 9.8897 ± 0.0004 Å
• c: 20.4731 ± 0.0007 Å
• α: 80.728 ± 0.002°
• β: 77.828 ± 0.002°
• γ: 83.623 ± 0.002°
• Cell volume: 1780.12 ± 0.11 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0221
• Residual factor for significantly intense reflections: 0.0208
• Weighted residual factors for significantly intense reflections: 0.0436
• Weighted residual factors for all reflections included in the refinement: 0.0441
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No