Information card for entry 4088856

Structure parameters

• Formula: C9 H18 Cl3 Ga O3 Os P2
• Calculated formula: C9 H18 Cl3 Ga O3 Os P2
• SMILES: [Os]([Ga](Cl)(Cl)Cl)(C#[O])([P](C)(C)C)(C#[O])([P](C)(C)C)C#[O]
• Title of publication: Metal-Only Lewis Pairs Based on Zerovalent Osmium
• Authors of publication: Bissert, Robin; Braunschweig, Holger; Dewhurst, Rian D.; Schneider, Christoph
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 15
• Pages of publication: 2567
• a: 8.983 ± 0.0012 Å
• b: 12.9064 ± 0.0019 Å
• c: 19.16 ± 0.003 Å
• α: 90°
• β: 97.911 ± 0.004°
• γ: 90°
• Cell volume: 2200.2 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0188
• Residual factor for significantly intense reflections: 0.0171
• Weighted residual factors for significantly intense reflections: 0.0445
• Weighted residual factors for all reflections included in the refinement: 0.046
• Goodness-of-fit parameter for all reflections included in the refinement: 1.043
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No