Crystallography Open Database

Information card for entry 4089032

Preview

Coordinates	4089032.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31 H53 Al N4
Calculated formula	C31 H53 Al N4
Title of publication	Aluminum and Gallium Hydrazides as Active Lewis Pairs: Cooperative C‒H Bond Activation with H‒C≡C‒Ph and Pentafluorobenzene
Authors of publication	Uhl, Werner; Willeke, Matthias; Hengesbach, Frank; Hepp, Alexander; Layh, Marcus
Journal of publication	Organometallics
Year of publication	2016
Journal volume	35
Journal issue	21
Pages of publication	3701
a	11.2344 ± 0.0014 Å
b	11.2633 ± 0.0014 Å
c	12.9804 ± 0.0017 Å
α	93.348 ± 0.004°
β	105.684 ± 0.003°
γ	111.948 ± 0.003°
Cell volume	1443.2 ± 0.3 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0788
Residual factor for significantly intense reflections	0.0652
Weighted residual factors for significantly intense reflections	0.1758
Weighted residual factors for all reflections included in the refinement	0.1876
Goodness-of-fit parameter for all reflections included in the refinement	1.026
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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