Information card for entry 4089061

Structure parameters

• Formula: C33 H47 B10 N4 O2 P
• Calculated formula: C33 H47 B10 N4 O2 P
• Title of publication: Nucleophilicity of Oximes Based upon Addition to a Nitriliumcloso-Decaborate Cluster
• Authors of publication: Bolotin, Dmitrii S.; Burianova, Valeria K.; Novikov, Alexander S.; Demakova, Marina Ya.; Pretorius, Carla; Mokolokolo, Pennie Petrus; Roodt, Andreas; Bokach, Nadezhda A.; Suslonov, Vitaliy V.; Zhdanov, Andrey P.; Zhizhin, Konstantin Yu.; Kuznetsov, Nikolay T.; Kukushkin, Vadim Yu.
• Journal of publication: Organometallics
• Year of publication: 2016
• Journal volume: 35
• Journal issue: 20
• Pages of publication: 3612
• a: 9.9583 ± 0.0003 Å
• b: 12.4732 ± 0.0004 Å
• c: 15.1134 ± 0.0005 Å
• α: 75.084 ± 0.003°
• β: 85.019 ± 0.003°
• γ: 84.536 ± 0.003°
• Cell volume: 1801.97 ± 0.1 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0806
• Residual factor for significantly intense reflections: 0.0795
• Weighted residual factors for significantly intense reflections: 0.1638
• Weighted residual factors for all reflections included in the refinement: 0.1642
• Goodness-of-fit parameter for all reflections included in the refinement: 1.283
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No