Information card for entry 4089247

Structure parameters

• Formula: C32 H76 N2 O8 Si8 Yb
• Calculated formula: C32 H76 N2 O8 Si8 Yb
• SMILES: [Yb]12([Si]([Si](C)(C)C)([Si]34[O]1CCN(CCO3)CCO4)[Si](C)(C)C)([Si]([Si]13[O]2CCN(CCO3)CCO1)([Si](C)(C)C)[Si](C)(C)C)([O]1CCCC1)[O]1CCCC1
• Title of publication: Tuning the Si-N Interaction in Metalated Oligosilanylsilatranes.
• Authors of publication: Aghazadeh Meshgi, Mohammad; Zitz, Rainer; Walewska, Małgorzata; Baumgartner, Judith; Marschner, Christoph
• Journal of publication: Organometallics
• Year of publication: 2017
• Journal volume: 36
• Journal issue: 7
• Pages of publication: 1365 - 1371
• a: 9.9691 ± 0.0012 Å
• b: 15.4589 ± 0.0019 Å
• c: 16.395 ± 0.002 Å
• α: 81.587 ± 0.003°
• β: 87.487 ± 0.002°
• γ: 86.698 ± 0.003°
• Cell volume: 2493.7 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.113
• Residual factor for significantly intense reflections: 0.0807
• Weighted residual factors for significantly intense reflections: 0.173
• Weighted residual factors for all reflections included in the refinement: 0.191
• Goodness-of-fit parameter for all reflections included in the refinement: 0.95
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No