Information card for entry 4089378

Structure parameters

• Common name: [L(tBu)Co(H)]2
• Formula: C76 H108 Co2 D6 N4
• Calculated formula: C76 H114 Co2 N4
• Title of publication: Low-Coordinate Cobalt Fluoride Complexes: Synthesis, Reactions, and Production from C‒F Activation Reactions
• Authors of publication: Dugan, Thomas R.; Goldberg, Jonathan M.; Brennessel, William W.; Holland, Patrick L.
• Journal of publication: Organometallics
• Year of publication: 2012
• Journal volume: 31
• Journal issue: 4
• Pages of publication: 1349
• a: 12.2671 ± 0.0006 Å
• b: 13.3398 ± 0.0007 Å
• c: 23.792 ± 0.0017 Å
• α: 98.582 ± 0.002°
• β: 94.212 ± 0.002°
• γ: 117.175 ± 0.001°
• Cell volume: 3380.1 ± 0.3 ų
• Cell temperature: 100 ± 0.1 K
• Ambient diffraction temperature: 100 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1096
• Residual factor for significantly intense reflections: 0.0621
• Weighted residual factors for significantly intense reflections: 0.1348
• Weighted residual factors for all reflections included in the refinement: 0.1576
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No