Information card for entry 4089529

Structure parameters

• Formula: C22 H29 O10 P3 W2
• Calculated formula: C22 H29 O10 P3 W2
• Title of publication: Versatile Reactivity of Bridged Pentelidene Complexes toward Secondary and Tertiary Phosphines
• Authors of publication: Stubenhofer, Markus; Kuntz, Christian; Bodensteiner, Michael; Timoshkin, Alexey Y.; Scheer, Manfred
• Journal of publication: Organometallics
• Year of publication: 2013
• Journal volume: 32
• Journal issue: 12
• Pages of publication: 3521
• a: 21.8086 ± 0.0002 Å
• b: 8.795 ± 0.0001 Å
• c: 16.1926 ± 0.0001 Å
• α: 90°
• β: 104.565 ± 0.001°
• γ: 90°
• Cell volume: 3006.04 ± 0.05 ų
• Cell temperature: 123 ± 1 K
• Ambient diffraction temperature: 123 ± 1 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0207
• Residual factor for significantly intense reflections: 0.0182
• Weighted residual factors for significantly intense reflections: 0.0439
• Weighted residual factors for all reflections included in the refinement: 0.0448
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No