Information card for entry 4089718

Structure parameters

• Common name: [Sn{(C(SiMe3)2SiMe2CH2)2}{O2C6H3(tBu)2}]
• Formula: C34 H72 O2 Si6 Sn
• Calculated formula: C34 H72 O2 Si6 Sn
• Title of publication: Reactions of a Highly Crowded Cyclic Stannylene with Iodoalkanes, Enones, and Dienes. Inhibition of Nucleophilic Substitution at Tin(IV) Centers
• Authors of publication: Asadi, Ashrafolmolouk; Eaborn, Colin; Hill, Michael S.; Hitchcock, Peter B.; Meehan, Margaret M.; Smith, J. David
• Journal of publication: Organometallics
• Year of publication: 2002
• Journal volume: 21
• Journal issue: 12
• Pages of publication: 2430
• a: 11.2943 ± 0.0002 Å
• b: 16.6702 ± 0.0003 Å
• c: 23.2637 ± 0.0004 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 4380.05 ± 0.13 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0394
• Residual factor for significantly intense reflections: 0.0331
• Weighted residual factors for significantly intense reflections: 0.069
• Weighted residual factors for all reflections included in the refinement: 0.0721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No