Information card for entry 4101464

Structure parameters

• Formula: C59 H106 P2 Pt
• Calculated formula: C58.992 H106 P2 Pt
• Title of publication: Gyroscope-like molecules consisting of PdX2/PtX2 rotators encased in three-spoke stators: synthesis via alkene metathesis, and facile substitution and demetalation.
• Authors of publication: Nawara, Agnieszka J; Shima, Takanori; Hampel, Frank; Gladysz, J A
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Journal issue: 15
• Pages of publication: 4962 - 4963
• a: 11.9863 ± 0.0002 Å
• b: 16.467 ± 0.0003 Å
• c: 16.9113 ± 0.0002 Å
• α: 67.387 ± 0.001°
• β: 72.547 ± 0.001°
• γ: 79.382 ± 0.001°
• Cell volume: 2930.44 ± 0.08 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 4
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0365
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0748
• Weighted residual factors for all reflections included in the refinement: 0.0792
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No