Information card for entry 4102058

Structure parameters

• Chemical name: [(u-N)(U(N[t-Bu][3,5-Me2C6H3])3)2][B(3,5-(CF3)2C6H3)4]
• Formula: C108 H128 B F24 N7 O U2
• Calculated formula: C108 H128 B F24 N7 O U2
• Title of publication: Uranium-Nitrogen Multiple Bonding: Isostructural Anionic, Neutral, and Cationic Uranium Nitride Complexes Featuring a Linear U=N=U Core
• Authors of publication: Alexander R. Fox; Polly L. Arnold; Christopher C. Cummins
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 3250 - 3251
• a: 14.138 ± 0.003 Å
• b: 14.224 ± 0.003 Å
• c: 27.716 ± 0.006 Å
• α: 104.253 ± 0.004°
• β: 94.05 ± 0.004°
• γ: 91.825 ± 0.004°
• Cell volume: 5382 ± 2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0789
• Residual factor for significantly intense reflections: 0.0401
• Weighted residual factors for significantly intense reflections: 0.0754
• Weighted residual factors for all reflections included in the refinement: 0.088
• Goodness-of-fit parameter for all reflections included in the refinement: 1.021
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No