Information card for entry 4102472

Structure parameters

• Formula: C35 H50 I2 N O3 Si2 U
• Calculated formula: C35 H50 I2 N O3 Si2 U
• SMILES: [U]1(I)(I)(O[Si](C)(C)C)(O[Si](C)(C)C)OC(=CC(=[N]1c1cc(cc(c1)C(C)(C)C)C(C)(C)C)c1ccccc1)c1ccccc1
• Title of publication: Oxo Ligand Silylation in a Uranyl β-Ketoiminate Complex
• Authors of publication: Jessie L. Brown; Guang Wu; Trevor W. Hayton
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 7248 - 7249
• a: 9.0488 ± 0.0006 Å
• b: 19.7697 ± 0.0013 Å
• c: 23.4059 ± 0.0015 Å
• α: 90°
• β: 94.775 ± 0.002°
• γ: 90°
• Cell volume: 4172.6 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0618
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.1064
• Weighted residual factors for all reflections included in the refinement: 0.1187
• Goodness-of-fit parameter for all reflections included in the refinement: 1.119
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No