Information card for entry 4103504

Structure parameters

• Chemical name: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.8 (release 12-01-2007 CrysAlis171 .NET) (compiled Jan 12 2007,17:49:11)
• Formula: C38 H58 N4 Ni O Si2
• Calculated formula: C38 H58 N4 Ni O Si2
• Title of publication: An Isolable Bis-Silylene Oxide ("Disilylenoxane") and Its Metal Coordination
• Authors of publication: Wenyuan Wang; Shigeyoshi Inoue; Shenglai Yao; Matthias Driess
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 15890 - 15892
• a: 9.8776 ± 0.0008 Å
• b: 12.953 ± 0.0011 Å
• c: 15.5488 ± 0.0013 Å
• α: 81.634 ± 0.007°
• β: 83.316 ± 0.007°
• γ: 82.826 ± 0.007°
• Cell volume: 1943 ± 0.3 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0605
• Residual factor for significantly intense reflections: 0.0386
• Weighted residual factors for significantly intense reflections: 0.0807
• Weighted residual factors for all reflections included in the refinement: 0.0853
• Goodness-of-fit parameter for all reflections included in the refinement: 0.948
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No