Information card for entry 4103506

Structure parameters

• Chemical name: CrysAlis RED, Oxford Diffraction Ltd., Version 1.171.31.8 (release 12-01-2007 CrysAlis171 .NET) (compiled Jan 12 2007,17:49:11)
• Formula: C30 H48 Cl2 N4 O Si2
• Calculated formula: C30 H48 Cl2 N4 O Si2
• Title of publication: An Isolable Bis-Silylene Oxide ("Disilylenoxane") and Its Metal Coordination
• Authors of publication: Wenyuan Wang; Shigeyoshi Inoue; Shenglai Yao; Matthias Driess
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2010
• Journal volume: 132
• Pages of publication: 15890 - 15892
• a: 12.1593 ± 0.0005 Å
• b: 16.2045 ± 0.0006 Å
• c: 17.1248 ± 0.0007 Å
• α: 90°
• β: 98.177 ± 0.004°
• γ: 90°
• Cell volume: 3339.9 ± 0.2 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0905
• Residual factor for significantly intense reflections: 0.0543
• Weighted residual factors for significantly intense reflections: 0.108
• Weighted residual factors for all reflections included in the refinement: 0.1194
• Goodness-of-fit parameter for all reflections included in the refinement: 1.035
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No