Information card for entry 4103999

Structure parameters

• Formula: C28 H21 Cl F3 O Sb
• Calculated formula: C28 H21 Cl F3 O Sb
• SMILES: [Sb]12(OC(c3c1cccc3)(c1c2cccc1)C(F)(F)F)(c1ccc(Cl)cc1)c1cc(cc(c1)C)C
• Title of publication: Pentacoordinate Organoantimony Compounds That Isomerize by Turnstile Rotation
• Authors of publication: Shiro Matsukawa; Hideaki Yamamichi; Yohsuke Yamamoto; Kaori Ando
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 3418 - 3419
• a: 8.418 ± 0.0002 Å
• b: 10.079 ± 0.0002 Å
• c: 14.748 ± 0.0004 Å
• α: 96.205 ± 0.001°
• β: 100.733 ± 0.001°
• γ: 93.319 ± 0.001°
• Cell volume: 1218.3 ± 0.05 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0397
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.1029
• Weighted residual factors for all reflections included in the refinement: 0.1038
• Goodness-of-fit parameter for all reflections included in the refinement: 1.096
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No