Information card for entry 4105106

Structure parameters

• Formula: C40 H62 B O P4 Rh S4
• Calculated formula: C40 H62 B O P4 Rh S4
• Title of publication: Thermodynamic Studies and Hydride Transfer Reactions from a Rhodium Complex to BX3 Compounds
• Authors of publication: Michael T. Mock; Robert G. Potter; Donald M. Camaioni; Jun Li; William G. Dougherty; W. Scott Kassel; Brendan Twamley; Daniel L. DuBois
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 14454 - 14465
• a: 13.0664 ± 0.0011 Å
• b: 13.0868 ± 0.0011 Å
• c: 13.553 ± 0.0012 Å
• α: 74.795 ± 0.003°
• β: 83.485 ± 0.003°
• γ: 89.799 ± 0.003°
• Cell volume: 2221.1 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0324
• Residual factor for significantly intense reflections: 0.026
• Weighted residual factors for significantly intense reflections: 0.06
• Weighted residual factors for all reflections included in the refinement: 0.0627
• Goodness-of-fit parameter for all reflections included in the refinement: 1.024
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No