Information card for entry 4105352

Structure parameters

• Formula: C56 H44 Cl16 N4 O18 Rh2
• Calculated formula: C56 H40 Cl16 N4 O18 Rh2
• Title of publication: Experimental Evidence for the All-Up Reactive Conformation of Chiral Rhodium(II) Carboxylate Catalysts: Enantioselective Synthesis of cis-Cyclopropane α-Amino Acids
• Authors of publication: Vincent N. G. Lindsay; Wei Lin; André B. Charette
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 16383 - 16385
• a: 22.3018 ± 0.0007 Å
• b: 22.3018 Å
• c: 21.439 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10663.1 ± 0.5 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 90
• Hermann-Mauguin space group symbol: P 4 21 2
• Hall space group symbol: P 4ab 2ab
• Residual factor for all reflections: 0.1177
• Residual factor for significantly intense reflections: 0.0877
• Weighted residual factors for significantly intense reflections: 0.2344
• Weighted residual factors for all reflections included in the refinement: 0.2546
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No