Information card for entry 4105403

Structure parameters

• Formula: C32.38 H32.75 Cl4.75 N2 O8 Pd2
• Calculated formula: C32.375 H32.75 Cl4.75 N2 O8 Pd2
• Title of publication: Bimetallic Palladium Catalysis: Direct Observation of Pd(III)-Pd(III) Intermediates
• Authors of publication: David C. Powers; Matthias A. L. Geibel; Johannes E. M. N. Klein; Tobias Ritter
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17050 - 17051
• a: 13.0941 ± 0.0019 Å
• b: 14.506 ± 0.002 Å
• c: 19.684 ± 0.003 Å
• α: 95.217 ± 0.002°
• β: 90.019 ± 0.002°
• γ: 95.349 ± 0.002°
• Cell volume: 3707 ± 0.9 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0608
• Residual factor for significantly intense reflections: 0.0433
• Weighted residual factors for significantly intense reflections: 0.0916
• Weighted residual factors for all reflections included in the refinement: 0.1012
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No