Information card for entry 4105450

Structure parameters

• Formula: C24 H44 Cl16 Ga4 P4
• Calculated formula: C24 H44 Cl16 Ga4 P4
• SMILES: [Ga](Cl)(Cl)(Cl)[Cl][Ga](Cl)(Cl)Cl.[Ga](Cl)(Cl)(Cl)[Cl][Ga](Cl)(Cl)Cl.Cl[P+]1(P([P+](Cl)(P1C1CCCCC1)C1CCCCC1)C1CCCCC1)C1CCCCC1
• Title of publication: New Synthetic Procedures to Catena-Phosphorus Cations: Preparation and Dissociation of the First cyclo-Phosphino-halophosphonium Salts
• Authors of publication: Jan J. Weigand; Neil Burford; Reagan J. Davidson; T. Stanley Cameron; Patrick Seelheim
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2009
• Journal volume: 131
• Pages of publication: 17943 - 17953
• a: 17.807 ± 0.0004 Å
• b: 17.9537 ± 0.0003 Å
• c: 31.5222 ± 0.0008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 10077.7 ± 0.4 ų
• Cell temperature: 123.1 K
• Ambient diffraction temperature: 123.1 ± 0.2 K
• Number of distinct elements: 5
• Space group number: 61
• Hermann-Mauguin space group symbol: P b c a
• Hall space group symbol: -P 2ac 2ab
• Residual factor for significantly intense reflections: 0.0478
• Weighted residual factors for all reflections included in the refinement: 0.0593
• Goodness-of-fit parameter for all reflections included in the refinement: 0.97
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No