Information card for entry 4105539

Structure parameters

• Chemical name: catena-(di(hexafluoroacetylacetonate)-iron(II)- di(hexafluoroacetylacetonate)-lead(II))
• Formula: C20 H4 F24 Fe O8 Pb
• Calculated formula: C20 H4 F24 Fe O8 Pb
• Title of publication: Fluorinated Heterometallic β-Diketonates as Volatile Single-Source Precursors for the Synthesis of Low-Valent Mixed-Metal Fluorides
• Authors of publication: Anantharamulu Navulla; Alexander A. Tsirlin; Artem M. Abakumov; Roman V. Shpanchenko; Haitao Zhang; Evgeny V. Dikarev
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 692 - 694
• a: 11.4406 ± 0.0006 Å
• b: 12.3702 ± 0.0007 Å
• c: 13.582 ± 0.0008 Å
• α: 65.896 ± 0.001°
• β: 66.64 ± 0.001°
• γ: 64.316 ± 0.001°
• Cell volume: 1523.87 ± 0.15 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0418
• Residual factor for significantly intense reflections: 0.0384
• Weighted residual factors for significantly intense reflections: 0.0964
• Weighted residual factors for all reflections included in the refinement: 0.0991
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No