Information card for entry 4105787

Structure parameters

• Formula: C39 H98 N6 O2 Si8 Y2
• Calculated formula: C39 H88 N6 O2 Si8 Y2
• Title of publication: Synthesis of the (N2)3- Radical from Y2+ and Its Protonolysis Reactivity To Form (N2H2)2- via the Y[N(SiMe3)2]3/KC8 Reduction System
• Authors of publication: Ming Fang; David S. Lee; Joseph W. Ziller; Robert J. Doedens; Jefferson E. Bates; Filipp Furche; William J. Evans
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 3784 - 3787
• a: 11.6254 ± 0.0012 Å
• b: 12.3668 ± 0.0012 Å
• c: 12.9283 ± 0.0013 Å
• α: 102.254 ± 0.001°
• β: 110.145 ± 0.001°
• γ: 110.139 ± 0.001°
• Cell volume: 1518.5 ± 0.3 ų
• Cell temperature: 153 ± 2 K
• Ambient diffraction temperature: 153 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0584
• Residual factor for significantly intense reflections: 0.0423
• Weighted residual factors for significantly intense reflections: 0.1077
• Weighted residual factors for all reflections included in the refinement: 0.1169
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No