Crystallography Open Database

Information card for entry 4105877

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Coordinates	4105877.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	dichlorotetragermetene
Formula	C36 H84 Cl2 Ge4 Si4
Calculated formula	C36 H84 Cl2 Ge4 Si4
Title of publication	From Tetragermacyclobutene to Tetragermacyclobutadiene Dianion to Tetragermacyclobutadiene Transition Metal Complexes
Authors of publication	Vladimir Ya. Lee; Yuki Ito; Hiroyuki Yasuda; Kazunori Takanashi; Akira Sekiguchi
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	5103 - 5108
a	41.297 ± 0.0009 Å
b	15.666 ± 0.0007 Å
c	17.271 ± 0.0007 Å
α	90°
β	112.773 ± 0.002°
γ	90°
Cell volume	10302.6 ± 0.7 Å³
Cell temperature	150 K
Ambient diffraction temperature	150 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0613
Residual factor for significantly intense reflections	0.0432
Weighted residual factors for significantly intense reflections	0.1108
Weighted residual factors for all reflections included in the refinement	0.1203
Goodness-of-fit parameter for all reflections included in the refinement	0.997
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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