Information card for entry 4105944

Structure parameters

• Formula: C48 H106 K N O6 Si10 Sn
• Calculated formula: C48 H106 K N O6 Si10 Sn
• SMILES: [Sn]1([Si]([Si]([Si]([Si]1([Si](C)(C)C)[Si](C)(C)C)(C)C)(C)C)([Si](C)(C)C)[Si](C)(C)C)N([Si](C)(C)C)[Si](C)(C)C.[K]12345[O]6CC[O]1CC[O]2CC[O]3CC[O]4CC[O]5CC6.c1ccc(cc1)C.c1(ccccc1)C
• Title of publication: A Cyclic Disilylated Stannylene: Synthesis, Dimerization, and Adduct Formation
• Authors of publication: Henning Arp; Judith Baumgartner; Christoph Marschner; Thomas Müller
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 5632 - 5635
• a: 12.615 ± 0.003 Å
• b: 25.832 ± 0.005 Å
• c: 24.001 ± 0.005 Å
• α: 90°
• β: 94.39 ± 0.03°
• γ: 90°
• Cell volume: 7798 ± 3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.2316
• Residual factor for significantly intense reflections: 0.1566
• Weighted residual factors for significantly intense reflections: 0.3458
• Weighted residual factors for all reflections included in the refinement: 0.3889
• Goodness-of-fit parameter for all reflections included in the refinement: 1.065
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No