Information card for entry 4106943

Structure parameters

• Formula: C46 H87 Ge N7 O P2 Si
• Calculated formula: C46 H87 Ge N7 O P2 Si
• Title of publication: Synthesis and Reactivity of a Phosphine-Stabilized Monogermanium Analogue of Alkynes
• Authors of publication: Juliette Berthe; Juan Manuel Garcia; Edgar Ocando; Tsuyoshi Kato; Nathalie Saffon-Merceron; Abel De Cózar; Fernando P. Cossío; Antoine Baceiredo
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 15930 - 15933
• a: 10.4194 ± 0.0003 Å
• b: 13.8223 ± 0.0006 Å
• c: 20.0405 ± 0.0005 Å
• α: 76.492 ± 0.001°
• β: 75.028 ± 0.001°
• γ: 82.15 ± 0.002°
• Cell volume: 2702.18 ± 0.16 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0439
• Residual factor for significantly intense reflections: 0.0361
• Weighted residual factors for significantly intense reflections: 0.0963
• Weighted residual factors for all reflections included in the refinement: 0.1013
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No