Crystallography Open Database

Information card for entry 4107048

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Coordinates	4107048.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C154.8 H121.8 B4 F60 N8 O6 Si4
Calculated formula	C154.8 H121.8 B4 F60 N8 O6 Si4
Title of publication	Donor-Acceptor-Stabilized Silicon Analogue of an Acid Anhydride
Authors of publication	Rajendra S. Ghadwal; Ramachandran Azhakar; Herbert W. Roesky; Kevin Pröpper; Birger Dittrich; Susanne Klein; Gernot Frenking
Journal of publication	Journal of the American Chemical Society
Year of publication	2011
Journal volume	133
Pages of publication	17552 - 17555
a	13.3606 ± 0.0002 Å
b	13.8311 ± 0.0002 Å
c	21.853 ± 0.0004 Å
α	77.852 ± 0.001°
β	74.896 ± 0.001°
γ	77.025 ± 0.001°
Cell volume	3749.34 ± 0.11 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.0515
Weighted residual factors for significantly intense reflections	0.1401
Weighted residual factors for all reflections included in the refinement	0.1522
Goodness-of-fit parameter for all reflections included in the refinement	1.049
Diffraction radiation wavelength	1.54178 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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