Information card for entry 4107141

Structure parameters

• Formula: C61 H86 Ag Ge3 I P6 Pd4
• Calculated formula: C61 H86 Ag Ge3 I P6 Pd4
• SMILES: I[Ag]1[Pd]23456[Pd]781([Ge]5([Pd]13([Ge]4([Pd]32([Ge]67(c2ccccc2)c2ccccc2)[P](C)(C)CC[P]3(C)C)(c2ccccc2)c2ccccc2)[P](C)(C)CC[P]1(C)C)(c1ccccc1)c1ccccc1)[P](C)(C)CC[P]8(C)C.Cc1ccccc1
• Title of publication: Tetrapalladium Complex with Bridging Germylene Ligands. Structural Change of the Planar Pd4Ge3 Core
• Authors of publication: Makoto Tanabe; Naoko Ishikawa; Mai Chiba; Tomohito Ide; Kohtaro Osakada; Tomoaki Tanase
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2011
• Journal volume: 133
• Pages of publication: 18598 - 18601
• a: 13.443 ± 0.003 Å
• b: 18.101 ± 0.004 Å
• c: 28.587 ± 0.006 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6956 ± 3 ų
• Cell temperature: 113.1 K
• Ambient diffraction temperature: 113.1 K
• Number of distinct elements: 7
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0743
• Residual factor for significantly intense reflections: 0.0636
• Weighted residual factors for significantly intense reflections: 0.1344
• Weighted residual factors for all reflections included in the refinement: 0.1406
• Goodness-of-fit parameter for all reflections included in the refinement: 1.099
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No