Information card for entry 4107598

Structure parameters

• Common name: Tip3Ph2-Cyclotrisilanid
• Chemical name: rac-1,2,2-Tris(2,4,6-triisopropylpheny)-3,3-phenylcyclotrisilanid
• Formula: C64 H96 Li O Si3
• Calculated formula: C64 H96 Li O Si3
• Title of publication: Syntheses of Trisila Analogues of Allyl Chlorides and Their Transformations to Chlorocyclotrisilanes, Cyclotrisilanides, and a Trisilaindane
• Authors of publication: Kai Abersfelder; David Scheschkewitz
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2008
• Journal volume: 130
• Pages of publication: 4114 - 4121
• a: 12.9877 ± 0.0009 Å
• b: 13.6085 ± 0.001 Å
• c: 19.7857 ± 0.0014 Å
• α: 99.423 ± 0.002°
• β: 100.153 ± 0.002°
• γ: 112.956 ± 0.001°
• Cell volume: 3063.6 ± 0.4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0661
• Residual factor for significantly intense reflections: 0.0524
• Weighted residual factors for significantly intense reflections: 0.1235
• Weighted residual factors for all reflections included in the refinement: 0.1307
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No