Crystallography Open Database

Information card for entry 4110442

Preview

Coordinates	4110442.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C19 H41 P5 Ru
Calculated formula	C19 H41 P5 Ru
SMILES	[RuH]12(P(C)c3ccccc3)([P](CC[P]1(C)C)(C)C)[P](CC[P]2(C)C)(C)C
Title of publication	Asymmetric Catalytic Synthesis of P-Stereogenic Phosphines via a Nucleophilic Ruthenium Phosphido Complex
Authors of publication	Vincent S. Chan; Ian C. Stewart; Robert G. Bergman; F. Dean Toste
Journal of publication	Journal of the American Chemical Society
Year of publication	2006
Journal volume	128
Pages of publication	2786 - 2787
a	9.448 ± 0.0007 Å
b	15.478 ± 0.001 Å
c	17.141 ± 0.001 Å
α	90°
β	94.165 ± 0.001°
γ	90°
Cell volume	2500 ± 0.3 Å³
Cell temperature	120.2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for significantly intense reflections	0.0335
Weighted residual factors for all reflections included in the refinement	0.0363
Goodness-of-fit parameter for all reflections included in the refinement	1.295
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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