Information card for entry 4110816

Structure parameters

• Common name: Cp*V(B3H8)2
• Chemical name: Bis(octahydrotriborato)(pentamethycyclopentadienyl)vanadium(III)
• Formula: C10 H31 B6 V
• Calculated formula: C10 H31 B6 V
• Title of publication: Synthesis and Characterization of the Octahydrotriborate Complexes Cp*V(B3H8)2 and Cp*Cr(B3H8)2 and the Unusual Cobaltaborane Cluster Cp*2Co2(B6H14)
• Authors of publication: Do Young Kim; Gregory S. Girolami
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Pages of publication: 10969 - 10977
• a: 7.745 ± 0.003 Å
• b: 16.065 ± 0.006 Å
• c: 7.513 ± 0.003 Å
• α: 90°
• β: 116.825 ± 0.005°
• γ: 90°
• Cell volume: 834.2 ± 0.6 ų
• Cell temperature: 193 ± 2 K
• Ambient diffraction temperature: 193 ± 2 K
• Number of distinct elements: 4
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0989
• Residual factor for significantly intense reflections: 0.0697
• Weighted residual factors for significantly intense reflections: 0.1803
• Weighted residual factors for all reflections included in the refinement: 0.191
• Goodness-of-fit parameter for all reflections included in the refinement: 1.115
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No