Information card for entry 4111079

Structure parameters

• Chemical name: catena-((3,3-bis-methyl-1,3-selenasiletane) -dirhodium(ii)-tetratrifluoroacetate)
• Formula: C12 H10 F12 O8 Rh2 Se Si
• Calculated formula: C12 H10 F11.94 O8 Rh2 Se Si
• Title of publication: Synthesis, Structure, and Chemistry of New, Mixed Group 14 and 16 Heterocycles: Nucleophile-Induced Ring Contraction of Mesocyclic Dications
• Authors of publication: Eric Block; Evgeny V. Dikarev; Richard S. Glass; Jin Jin; Bo Li; Xiaojie Li; Shao-Zhong Zhang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2006
• Journal volume: 128
• Pages of publication: 14949 - 14961
• a: 9.5735 ± 0.0007 Å
• b: 11.3637 ± 0.0008 Å
• c: 13.0078 ± 0.0009 Å
• α: 65.779 ± 0.001°
• β: 73.406 ± 0.001°
• γ: 80.72 ± 0.001°
• Cell volume: 1235.23 ± 0.15 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0555
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.106
• Weighted residual factors for all reflections included in the refinement: 0.1138
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No