Information card for entry 4111612

Structure parameters

• Formula: C35 H37 Cl4 F6 N2 O2 Pd Sb
• Calculated formula: C35 H37 Cl4 F6 N2 O2 Pd Sb
• Title of publication: Reactions of Vinyl Acetate and Vinyl Trifluoroacetate with Cationic Diimine Pd(II) and Ni(II) Alkyl Complexes: Identification of Problems Connected with Copolymerizations of These Monomers with Ethylene
• Authors of publication: B. Scott Williams; Mark D. Leatherman; Peter S. White; Maurice Brookhart
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2005
• Journal volume: 127
• Pages of publication: 5132 - 5146
• a: 8.8149 ± 0.0009 Å
• b: 12.7183 ± 0.0013 Å
• c: 18.3693 ± 0.0019 Å
• α: 91.953 ± 0.001°
• β: 90.798 ± 0.002°
• γ: 108.682 ± 0.002°
• Cell volume: 1949.1 ± 0.3 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.073
• Residual factor for significantly intense reflections: 0.057
• Weighted residual factors for all reflections: 0.084
• Weighted residual factors for significantly intense reflections: 0.076
• Goodness-of-fit parameter for all reflections included in the refinement: 2.56
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MolybdenumKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No