Information card for entry 4112183

Structure parameters

• Common name: {[(DAniF)2Rh2]4(O12C44H44)2(OEt2)(CH3CN)4}*10(CH3CN)
• Formula: C240 H260 N30 O41 Rh8
• Calculated formula: C240 H232 N30 O41 Rh8
• Title of publication: A Calix[4]arene Carceplex with Four Rh24+ Fasteners
• Authors of publication: F. Albert Cotton; Peng Lei; Chun Lin; Carlos A. Murillo; Xiaoping Wang; Shu-Yan Yu; Zhong-Xing Zhang
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 1518 - 1525
• a: 17.577 ± 0.002 Å
• b: 19.64 ± 0.003 Å
• c: 19.871 ± 0.003 Å
• α: 69.092 ± 0.002°
• β: 69.336 ± 0.003°
• γ: 85.822 ± 0.003°
• Cell volume: 5984.7 ± 1.5 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1683
• Residual factor for significantly intense reflections: 0.0879
• Weighted residual factors for significantly intense reflections: 0.201
• Weighted residual factors for all reflections included in the refinement: 0.2363
• Goodness-of-fit parameter for all reflections included in the refinement: 1.127
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No