Crystallography Open Database

Information card for entry 4112381

Preview

Coordinates	4112381.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C46 H31 B F21 N P2 W
Calculated formula	C46 H31 B F21 N P2 W
Title of publication	Synthons for Coordinatively Unsaturated Complexes of Tungsten, and Their Use for the Synthesis of High Oxidation-State Silylene Complexes
Authors of publication	Benjamin V. Mork; T. Don Tilley
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	4375 - 4385
a	12.822 ± 0.001 Å
b	14.878 ± 0.001 Å
c	15.005 ± 0.001 Å
α	114.902 ± 0.001°
β	110.473 ± 0.001°
γ	94.868 ± 0.001°
Cell volume	2339.8 ± 0.3 Å³
Cell temperature	115 ± 1 K
Ambient diffraction temperature	115 ± 1 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0626
Residual factor for significantly intense reflections	0.0461
Weighted residual factors for all reflections	0.1171
Weighted residual factors for significantly intense reflections	0.1096
Goodness-of-fit parameter for all reflections	1.076
Goodness-of-fit parameter for significantly intense reflections	1.118
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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