Information card for entry 4112474

Structure parameters

• Common name: [Dipp*Ge(PhC=CPh)GeDipp*].1.5n-hexane.0.17methylcyclopentane
• Formula: C84 H107.38 Ge2
• Calculated formula: C83.9933 H84 Ge2
• Title of publication: Reactivity of Ar'GeGeAr' (Ar' = C6H3-2,6-Dipp2, Dipp = C6H3-2,6-iPr2) toward Alkynes: Isolation of a Stable Digermacyclobutadiene
• Authors of publication: Chunming Cui; Marilyn M. Olmstead; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 5062 - 5063
• a: 43.91 ± 0.007 Å
• b: 43.91 ± 0.007 Å
• c: 19.208 ± 0.007 Å
• α: 90°
• β: 90°
• γ: 120°
• Cell volume: 32073 ± 14 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 3
• Space group number: 148
• Hermann-Mauguin space group symbol: R -3 :H
• Hall space group symbol: -R 3
• Residual factor for all reflections: 0.0767
• Residual factor for significantly intense reflections: 0.0586
• Weighted residual factors for significantly intense reflections: 0.1565
• Weighted residual factors for all reflections included in the refinement: 0.1705
• Goodness-of-fit parameter for all reflections included in the refinement: 1.044
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No