Information card for entry 4112615

Structure parameters

• Common name: [Dipp*Ge(NSiMe3)]2.n-hexane
• Formula: C72 H106 Ge2 N2 Si2
• Calculated formula: C72 H92 Ge2 N2 Si2
• Title of publication: Synthesis and Characterization of the Non-Kekulé, Singlet Biradicaloid Ar'Ge(μ-NSiMe3)2GeAr' (Ar' = 2,6-Dipp2C6H3, Dipp = 2,6-i-Pr2C6H3)
• Authors of publication: Chunming Cui; Marcin Brynda; Marilyn M. Olmstead; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 6510 - 6511
• a: 23.9746 ± 0.0016 Å
• b: 11.6981 ± 0.0007 Å
• c: 25.186 ± 0.002 Å
• α: 90°
• β: 107.243 ± 0.004°
• γ: 90°
• Cell volume: 6746.1 ± 0.8 ų
• Cell temperature: 91 ± 2 K
• Ambient diffraction temperature: 91 ± 2 K
• Number of distinct elements: 5
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0619
• Residual factor for significantly intense reflections: 0.0385
• Weighted residual factors for significantly intense reflections: 0.092
• Weighted residual factors for all reflections included in the refinement: 0.1056
• Goodness-of-fit parameter for all reflections included in the refinement: 1.062
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No