Crystallography Open Database

Information card for entry 4112709

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Coordinates	4112709.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H38 Ni P2 Si3
Calculated formula	C22 H34.92 Ni P2 Si3
Title of publication	Reaction of [2-(SiH3)C6H4]2SiH2 with Ni(Et2PCH2CH2PEt2)(PEt3)2: Characterization of η2-(Si-H)Ni and NiIV-H Complexes
Authors of publication	Wanzhi Chen; Shigeru Shimada; Masato Tanaka; Yuka Kobayashi; Kazuhiko Saigo
Journal of publication	Journal of the American Chemical Society
Year of publication	2004
Journal volume	126
Pages of publication	8072 - 8073
a	9.2218 ± 0.0004 Å
b	14.3152 ± 0.0006 Å
c	9.8666 ± 0.0004 Å
α	90°
β	101.799 ± 0.001°
γ	90°
Cell volume	1274.99 ± 0.09 Å³
Cell temperature	113 ± 2 K
Ambient diffraction temperature	113 ± 2 K
Number of distinct elements	5
Space group number	4
Hermann-Mauguin space group symbol	P 1 21 1
Hall space group symbol	P 2yb
Residual factor for significantly intense reflections	0.027
Weighted residual factors for all reflections included in the refinement	0.069
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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