Information card for entry 4112813

Structure parameters

• Chemical name: Tetrakis(tetrahydrofuran)lithium(I) 1,1,4,4-tetra-tert-butyl -2,3-Tetrakis[di-tert-butyl(methyl)silyl]-1,4-dimethyltetrasilane-2-yl-3-ide
• Formula: C52 H116 Li O4 Si6
• Calculated formula: C52 H116 Li O4 Si6
• Title of publication: Isolable Anion Radical of Blue Disilene (tBu2MeSi)2SiSi(SiMetBu2)2 Formed upon One-Electron Reduction: Synthesis and Characterization
• Authors of publication: Akira Sekiguchi; Shigeyoshi Inoue; Masaaki Ichinohe; Yoriko Arai
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 9626 - 9629
• a: 12.072 ± 0.0003 Å
• b: 21.567 ± 0.001 Å
• c: 24.25 ± 0.0011 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6313.7 ± 0.4 ų
• Cell temperature: 200 ± 0.1 K
• Ambient diffraction temperature: 200 ± 0.1 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0671
• Residual factor for significantly intense reflections: 0.0526
• Weighted residual factors for significantly intense reflections: 0.1388
• Weighted residual factors for all reflections included in the refinement: 0.1514
• Goodness-of-fit parameter for all reflections included in the refinement: 1.027
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No