Information card for entry 4112868

Structure parameters

• Formula: C22 H37 Mo P2 Si
• Calculated formula: C22 H37 Mo P2 Si
• Title of publication: Silylene Hydride Complexes of Molybdenum with Silicon-Hydrogen Interactions: Neutron Structure of (η5-C5Me5)(Me2PCH2CH2PMe2)Mo(H)(SiEt2)
• Authors of publication: Benjamin V. Mork; T. Don Tilley; Arthur J. Schultz; John A. Cowan
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 10428 - 10440
• a: 14.1108 ± 0.0002 Å
• b: 12.2418 ± 0.0003 Å
• c: 14.0009 ± 0.0001 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2418.54 ± 0.07 ų
• Cell temperature: 143 ± 1 K
• Ambient diffraction temperature: 143 ± 1 K
• Number of distinct elements: 5
• Space group number: 62
• Hermann-Mauguin space group symbol: P n m a
• Hall space group symbol: -P 2ac 2n
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for all reflections: 0.0798
• Weighted residual factors for significantly intense reflections: 0.0759
• Goodness-of-fit parameter for all reflections: 0.911
• Goodness-of-fit parameter for significantly intense reflections: 0.978
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No