Information card for entry 4112898

Structure parameters

• Formula: C60 H65 B F24 Ni P2
• Calculated formula: C60 H65 B F24 Ni P2
• Title of publication: Preparation of Stable Alkyl Complexes of Ni(I) and Their One-Electron Oxidation to Ni(II) Complex Cations
• Authors of publication: Kristina D. Kitiachvili; Daniel J. Mindiola; Gregory L. Hillhouse
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 10554 - 10555
• a: 35.135 ± 0.003 Å
• b: 12.723 ± 0.0011 Å
• c: 13.4387 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 6007.4 ± 0.9 ų
• Cell temperature: 373 ± 2 K
• Ambient diffraction temperature: 100 K
• Number of distinct elements: 6
• Space group number: 33
• Hermann-Mauguin space group symbol: P n a 21
• Hall space group symbol: P 2c -2n
• Residual factor for all reflections: 0.0637
• Residual factor for significantly intense reflections: 0.0579
• Weighted residual factors for significantly intense reflections: 0.1283
• Weighted residual factors for all reflections included in the refinement: 0.1317
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No