Information card for entry 4112900

Structure parameters

• Common name: [Li(THF)3(Et2O)][Li(HGeDipp*)2]
• Formula: C76 H98 Ge2 Li2 O4
• Calculated formula: C78 H98 Ge2 Li2 O4
• Title of publication: Reduction of Digermenes with Alkali Metals: Salts of Formula M2[{Ge(H)Ar'}2] (M = Li, Na, or K, Ar' = Terphenyl) with Three Different Structures
• Authors of publication: Anne F. Richards; Marcin Brynda; Philip P. Power
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2004
• Journal volume: 126
• Pages of publication: 10530 - 10531
• a: 18.6448 ± 0.0014 Å
• b: 17.6953 ± 0.0014 Å
• c: 12.6498 ± 0.001 Å
• α: 90°
• β: 114.431 ± 0.001°
• γ: 90°
• Cell volume: 3799.8 ± 0.5 ų
• Cell temperature: 91 ± 2 K
• Ambient diffraction temperature: 91 ± 2 K
• Number of distinct elements: 5
• Space group number: 12
• Hermann-Mauguin space group symbol: C 1 2/m 1
• Hall space group symbol: -C 2y
• Residual factor for all reflections: 0.0996
• Residual factor for significantly intense reflections: 0.0866
• Weighted residual factors for significantly intense reflections: 0.2484
• Weighted residual factors for all reflections included in the refinement: 0.2612
• Goodness-of-fit parameter for all reflections included in the refinement: 1.092
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No