Information card for entry 4113407

Structure parameters

• Formula: C50 H58 B Cl5 F4 O Os P2 Si2
• Calculated formula: C50 H58 B Cl5 F4 O Os P2 Si2
• Title of publication: Protonation and Bromination of an Osmabenzyne: Reactions Leading to the Formation of New Metallabenzynes
• Authors of publication: Ting Bin Wen; Sze Ming Ng; Wai Yiu Hung; Zhong Yuan Zhou; Man Fung Lo; Lai-Yung Shek; Ian D. Williams; Zhenyang Lin; Guochen Jia
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 884 - 885
• a: 12.1352 ± 0.0015 Å
• b: 13.9997 ± 0.0016 Å
• c: 17.118 ± 0.002 Å
• α: 80.135 ± 0.003°
• β: 78.298 ± 0.002°
• γ: 88.082 ± 0.002°
• Cell volume: 2805.6 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 9
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.052
• Residual factor for significantly intense reflections: 0.0402
• Weighted residual factors for significantly intense reflections: 0.1025
• Weighted residual factors for all reflections included in the refinement: 0.1081
• Goodness-of-fit parameter for all reflections included in the refinement: 0.994
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No