Crystallography Open Database

Information card for entry 4113526

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Coordinates	4113526.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C22 H37 I3 N11 Tm
Calculated formula	C22 H37 I3 N11 Tm
Title of publication	A Novel Bis(imino)amine Ligand as a Result of Acetonitrile Coupling with the Diiodides of Dy(II) and Tm(II)
Authors of publication	Mikhail N. Bochkarev; Georgii V. Khoroshenkov; Herbert Schumann; Sebastian Dechert
Journal of publication	Journal of the American Chemical Society
Year of publication	2003
Journal volume	125
Pages of publication	2894 - 2895
a	10.7188 ± 0.0003 Å
b	13.7619 ± 0.0005 Å
c	14.0021 ± 0.0005 Å
α	69.641 ± 0.001°
β	89.732 ± 0.001°
γ	73.989 ± 0.001°
Cell volume	1851.75 ± 0.11 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0832
Residual factor for significantly intense reflections	0.0499
Weighted residual factors for significantly intense reflections	0.0961
Weighted residual factors for all reflections included in the refinement	0.1061
Goodness-of-fit parameter for all reflections included in the refinement	1.016
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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