Information card for entry 4113987

Structure parameters

• Formula: C20 H49 Ge I Si4
• Calculated formula: C20 H49 Ge I Si4
• Title of publication: C-H Activation of Ethers and Alkanes by Germylene-Aryl Halide Complexes
• Authors of publication: Karla A. Miller; Jeffrey M. Bartolin; Rory M. O'Neill; Ryan D. Sweeder; Thomas M. Owens; Jeff W. Kampf; Mark M. Banaszak Holl; Norman J. Wells
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 8986 - 8987
• a: 10.2704 ± 0.0019 Å
• b: 11.857 ± 0.002 Å
• c: 12.554 ± 0.002 Å
• α: 86.381 ± 0.003°
• β: 82.483 ± 0.003°
• γ: 74.544 ± 0.003°
• Cell volume: 1460.2 ± 0.4 ų
• Cell temperature: 158 ± 2 K
• Ambient diffraction temperature: 158 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0188
• Residual factor for significantly intense reflections: 0.0178
• Weighted residual factors for significantly intense reflections: 0.0484
• Weighted residual factors for all reflections included in the refinement: 0.049
• Goodness-of-fit parameter for all reflections included in the refinement: 1.047
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No