Information card for entry 4114149

Structure parameters

• Common name: [Yb3(thf){Me3SiNCPhCHCPhNSiMe3}3]
• Formula: C67 H95 N6 O Si6 Yb3
• Calculated formula: C67 H95 N6 O Si6 Yb3
• Title of publication: Mono-, Di-, and Trianionic β-Diketiminato Ligands: A Computational Study and the Synthesis and Structure of [(YbL)3(THF)], L = [{N(SiMe3)C(Ph)}2CH]
• Authors of publication: Odile Eisenstein; Peter B. Hitchcock; Alexei V. Khvostov; Michael F. Lappert; Laurent Maron; Lionel Perrin; Andrey V. Protchenko
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 10790 - 10791
• a: 13.4823 ± 0.0004 Å
• b: 16.3546 ± 0.0005 Å
• c: 20.0818 ± 0.0006 Å
• α: 65.993 ± 0.002°
• β: 84.086 ± 0.002°
• γ: 86.355 ± 0.002°
• Cell volume: 4022.3 ± 0.2 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0546
• Residual factor for significantly intense reflections: 0.0388
• Weighted residual factors for significantly intense reflections: 0.1
• Weighted residual factors for all reflections included in the refinement: 0.1091
• Goodness-of-fit parameter for all reflections included in the refinement: 1.031
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No