Information card for entry 4114235

Structure parameters

• Common name: JDS-IV-16
• Chemical name: JDS-IV-16
• Formula: C19 H25 B Cl2 N7 Os
• Calculated formula: C19 H25 B Cl2 N7 Os
• Title of publication: Slow Hydrogen Atom Self-Exchange between Os(IV) Anilide and Os(III) Aniline Complexes: Relationships with Electron and Proton Transfer Self-Exchange
• Authors of publication: Jake D. Soper; James M. Mayer
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2003
• Journal volume: 125
• Pages of publication: 12217 - 12229
• a: 13.851 ± 0.0017 Å
• b: 8.624 ± 0.0011 Å
• c: 19.889 ± 0.003 Å
• α: 90°
• β: 107.515 ± 0.008°
• γ: 90°
• Cell volume: 2265.6 ± 0.5 ų
• Cell temperature: 130 ± 2 K
• Ambient diffraction temperature: 130 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1304
• Residual factor for significantly intense reflections: 0.0535
• Weighted residual factors for significantly intense reflections: 0.0891
• Weighted residual factors for all reflections included in the refinement: 0.1075
• Goodness-of-fit parameter for all reflections included in the refinement: 0.934
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No